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Synthesis of Chiral Phosphorus Reagents and Their Catalytic Activity in Asymmetric Borane Reduction of N-Phenyl Imine of Acetophenone
Eleven chiral trivalent or quatrivalent phosphorus reagents were synthesized starting from L-proline, D-camphor, (+)- or (-)-1,1′-binaphthalene-2,2′-diol, (-)-alpha-phenylethylamine, etc. and their application as catalysts in asymmetric borane reduction of N-phenyl imine of acetophenone was preliminary investigated. N-Phenyl alpha-phenylethylamine was obtained in good yield with low to moderate enantioselectivity.
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Reference£º
Chiral Catalysts,
Chiral catalysts – SlideShare