Reference of 33100-27-5. Let’s face it, organic chemistry can seem difficult to learn. Especially from a beginner’s point of view. Like 33100-27-5, Name is 1,4,7,10,13-Pentaoxacyclopentadecane. In a document type is Article, introducing its new discovery.
The reduction of 2,4,6-tri(4-pyridyl)-1,3,5-triazine (TPT) with alkali metals resulted in four radical anion salts (1, 2, 4 and 5) and one diradical dianion salt (3). Single-crystal X-ray diffraction and electron paramagnetic resonance (EPR) spectroscopy reveal that 1 contains the monoradical anion TPT.? stacked in one-dimensional (1D) with K+(18c6) and 2 can be viewed as a 1D magnetic chain of TPT.?, while 4 and 5 form radical metal-organic frameworks (RMOFs). 1D pore passages, with a diameter of 6.0 A, containing solvent molecules were observed in 5. Variable-temperature EPR measurements show that 3 has an open-shell singlet ground state that can be excited to a triplet state, consistent with theoretical calculation. The work suggests that the direct reduction approach could lead to the formation of RMOFs.
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