Introduction of a new synthetic route about 351498-10-7

With the rapid development of chemical substances, we look forward to future research findings about 351498-10-7

6,6′-((1E,1’E)-((2,3-Dimethylbutane-2,3-diyl)bis(azanylylidene))bis(methanylylidene))bis(2,4-di-tert-butylphenol), cas is 351498-10-7, it is a common heterocyclic compound, the chiral-catalyst compound, its synthesis route is as follows.,351498-10-7

N,N-Bis(3,5-di-tert-butylsalicylidene)-1 ,1 ,2,2-tetramethylethylenediamine (24, 0.73 g, 1 .3 mmol)was suspended in 10.0 mL of ethanol. The resulting suspension was heated to 80 c and stirred for 5minutes under argon balloon. Cobalt (II) acetate (0.24g, 1 .3 mmol) was then added, and the reactionmixture was stirred for another 2 hours at 80 00. The crimson red suspension was cooled down to roomtemperature in an ice bath and was filtered. The collected red solid was dried under vacuum to provide0.70 g of compound 25 (87%).

With the rapid development of chemical substances, we look forward to future research findings about 351498-10-7

Reference£º
Patent; SOLSTICE BIOLOGICS, LTD.; BRADSHAW, Curt, W.; SAKAMURI, Sukumar; LIU, Dingguo; (83 pag.)WO2016/94677; (2016); A2;,
Chiral Catalysts
Chiral catalysts – SlideShare