Reference of 14098-44-3. Let’s face it, organic chemistry can seem difficult to learn. Especially from a beginner’s point of view. Like 14098-44-3, Name is Benzo-15-crown-5. In a document type is Article, introducing its new discovery.
Reaction of NiCl2 · 6H2O, Na2[i-mnt] and benzo-15-crown-5 in CH3OHCH2Cl2 at room temperature leads to [{Na(benzo-15-crown-5)}2Ni(i-mnt)2]n · nCH2Cl2 (1). The same reaction with Na2[mnt] instead of Na2[i-mnt] affords [{Na(benzo-15-crown-5)}2Ni(mnt)2]n (2). Both complexes were isolated as crystalline products. X-ray diffraction analyses reveal that the main segments of 1 and 2 are infinite train structures, in which the building blocks Ni(i-mnt)2 or Ni(mnt)2 in end-to-end arrangements act as body frames and crown cycles standing by the body frames play the role of cartwheel. They are joined with each other through sodium ions.
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